Ra. Rao et al., DEPOSITION OF YBCO THIN-FILMS OVER LARGE AREAS BY A 90-DEGREES OFF-AXIS SPUTTERING TECHNIQUE, IEEE transactions on applied superconductivity, 7(2), 1997, pp. 1278-1282
We report the deposition of YBCO thin films with uniform thickness (<
+/- 5% variation), and stoichiometric composition (< 2.3% deviation fr
om the target stoichiometry) over an 8 '' diameter area, by a single t
arget 90 degrees off-axis sputtering technique using a 3 '' diameter t
arget and optimized substrate rotation, A 3 '' diameter resistive heat
er was used with optimized rotation in two consecutive deposition runs
to study the variation in film properties of small test samples depos
ited over an 8 '' diameter area, Due to the inherent temperature non-u
niformity of the heater, all the samples could not be deposited under
optimum growth conditions, However, all the films displayed a consiste
ntly high transition temperature (T-c > 87.5 degrees K) and critical c
urrent density (J(c) (77 K) > 1 x 10(6) A/cm(2), J(c) (4.2 K) > 1 x 10
(7) A/cm(2)) over an 8 '' diameter area, Considering only the better o
ptimized samples the films displayed high critical current densities (
J(c) (77 K) > 3 x 10(6) A/cm(2), J(c) (4.2 K) > 3 x 10(7) A/cm(2)). Th
e variations in the film properties have been correlated to the variat
ions in crystalline quality, amount of c-axis grains and substrate tem
perature during deposition.