Pp. Newcomer et al., MICROSTRUCTURAL CHANGES IN TLBA2CACU2O7-DELTA THIN-FILMS AFTER REDUCING ANNEALS WHICH ENHANCE CRITICAL-CURRENT DENSITY, IEEE transactions on applied superconductivity, 7(2), 1997, pp. 1887-1890
Microstructural changes in TlBa2CaCu2O7-partial derivative (Tl-1212) e
pitaxial thin films resulting from low oxygen partial pressure furnace
anneals at 600 degrees C are studied using high resolution transmissi
on electron microscopy (TEM), These postgrowth anneals have been shown
to significantly raise the superconducting transition temperature fro
m 70 to 90 K, and greatly improve the magnetic flux pinning and the cr
itical current density, Changes occur in both the microstructure and t
he morphology of the films that correlate with changes in J(c). Plan v
iew TEM and high-resolution cross-sectional TEM analysis of the films
before and after anneals demonstrates changes in the lattice fringe im
age, overall contrast modulation, and nanometer-scale discontinuities.