V. Beilin et al., DEFORMATION-DOMINATED TEXTURING OF SUPERCONDUCTING FILAMENT IN OPIT-FABRICATED BI(PB)SCCO-2223 AG COMPOSITE TAPES/, IEEE transactions on applied superconductivity, 7(2), 1997, pp. 2075-2078
Texture formation in the ceramic filament of Ag/BiSCCO tapes was studi
ed after cold rolling, uniaxial cold pressing and sintering by XRD --2
- and omega-scan methods, More effective texturing of the outer layers
as compared to that of the core interior was observed at the early ro
lling steps up to about 65% reduction in area, Texture inhomogeneity o
ver the filament cross section is related to the inhomogeneous distrib
ution of plastic deformation, Work hardening due to plastic deformatio
n of non-sintered powder results in the broadening of X-ray peaks and
an increase in microhardness. The recovery of these parameters occurs
after annealing at the temperatures of 350-600 degrees C. The omega-sc
an studies revealed an improvement of c-asis texture by intermediate r
olling compared to that in the omega-sintered and pressed states, Defo
rmation-induced texturing of the 2212-precursor is the main factor res
ponsible for the texture of the final 2223-phase, The influence of Ag
during the sintering stage is limited only to the outer levers of the
filament; in the case of low preliminary deformation internal layers r
emained practically non-oriented.