Cj. Eastell et al., TRANSMISSION ELECTRON-MICROSCOPY INVESTIGATION OF BI-BASED HTS TAPES, IEEE transactions on applied superconductivity, 7(2), 1997, pp. 2083-2086
Bi(Pb)-2223/Ag powder in tube tapes have been examined by TEM. The tap
es show good alignment and phase purity in the SEM but TEM investigati
ons revealed a number of fine-scale, current-limiting, features, Such
features include variation in grain boundary structure, amorphous phas
es at twist grain boundaries, residual 2212 layers present at grain bo
undaries and inside grains, and secondary phases, The Ag/superconducto
r interface has been shown to be relatively planar with no amorphous p
hases with the Bi(Pb)-2223 having near perfect c-axis alignment at the
interface.