The preparation of 3-substituted 1-chlorocarbonyl-imidazolidin-2-ones using bis(trichloromethyl) carbonate

Authors
Su, WK Zhang, YM
Citation
Wk. Su et Ym. Zhang, The preparation of 3-substituted 1-chlorocarbonyl-imidazolidin-2-ones using bis(trichloromethyl) carbonate, J CHEM R-S, (9), 2000, pp. 440-441
Citations number
22
Categorie Soggetti
Chemistry
Journal title
JOURNAL OF CHEMICAL RESEARCH-S
ISSN journal
03082342 → ACNP
Issue
9
Year of publication
2000
Pages
440 - 441
Database
ISI
SICI code
0308-2342(200009):9<440:TPO31U>2.0.ZU;2-N
Abstract
A novel synthesis of 3-substituted 1-chlorocarbonyl-imidazolidin-2-ones usi ng bis(trichloromethyl) carbonate is reported. The bis(trichloromethyl)carb onate is used to generate phosgene in situ in stoichiometric amounts. The y ields and purity of the products obtained are better than those obtained by a conventional way using phosgene.