Microbalance techniques in design and control of synthetic carbons

Citation
Am. Puziy et Oi. Poddubnaya, Microbalance techniques in design and control of synthetic carbons, J THERM ANA, 62(2), 2000, pp. 491-497
Citations number
20
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
ISSN journal
13886150 → ACNP
Volume
62
Issue
2
Year of publication
2000
Pages
491 - 497
Database
ISI
SICI code
1388-6150(2000)62:2<491:MTIDAC>2.0.ZU;2-G
Abstract
Peculiarities of carbonization of two styrene/divinylbenzene precursors (on e sulfonated, another aminated and phosphorylated) have been investigated b y thermogravimetry and differential thermal analysis. It was shown that pho sphorus compounds incorporate into carbon structure and cause delayed carbo nization. Porous structure and surface properties of synthetic carbons have been investigated by standard (BET, alpha (s) method, DA) and advanced (AE D, PSD, regularization) methods from benzene and water adsorption isotherms . It was shown that phosphorus-containing carbon is less microporous and sh ows highly hydrophilic surface.