A low-cost upgrade of a commercial magnetic resonance spectrometer to a broad-band system for NMR and ESR

Citation
P. Rosch et al., A low-cost upgrade of a commercial magnetic resonance spectrometer to a broad-band system for NMR and ESR, MEAS SCI T, 11(11), 2000, pp. 1610-1616
Citations number
10
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences","Instrumentation & Measurement
Journal title
MEASUREMENT SCIENCE & TECHNOLOGY
ISSN journal
09570233 → ACNP
Volume
11
Issue
11
Year of publication
2000
Pages
1610 - 1616
Database
ISI
SICI code
0957-0233(200011)11:11<1610:ALUOAC>2.0.ZU;2-8
Abstract
Due to their longevity and availability pulsed magnetic resonance spectrome ters of the types Bruker CXP and Bruker MSL are widely used in research ins titutions. This contribution gives a detailed description of how to extend these spectrometers to broad-band systems for NMR and ESR measurements. As it is based on off-the-shelf components, the approach reported here is both cost and time effective. Experimental results for a magnetically ordered i ntermetallic compound and a one-dimensional organic conductor demonstrate t he performance of the system. Particular attention is paid to the calibrati on procedure.