Na2Fe(CN)(5)(NO)center dot 2D(2)O at 11 and 293 K by X-ray, and at 15 K byneutron diffraction

Authors
Schultz, AJ Figgis, BN Sobolev, AN
Citation
Aj. Schultz et al., Na2Fe(CN)(5)(NO)center dot 2D(2)O at 11 and 293 K by X-ray, and at 15 K byneutron diffraction, ACT CRYST C, 56, 2000, pp. 1289-1291
Citations number
22
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
ISSN journal
01082701 → ACNP
Volume
56
Year of publication
2000
Part
11
Pages
1289 - 1291
Database
ISI
SICI code
0108-2701(200011)56:<1289:ND2A1A>2.0.ZU;2-H
Abstract
The crystal structure of Na2Fe(CN)(5)(NO). 2D(2)O, disodium pentacyanonitro sylferrate(III) bis(dideuterium oxide), has been determined by X-ray diffra ction at 11 and 293 K, and by neutron diffraction at 15 K. The accurate and extensive data sets lead to more precise determinations than are available from earlier work. The agreement in atomic positional and displacement par ameters between the determinations at low temperature is very good.