N. D'Souza et al., Directional and single-crystal solidification of Ni-base superalloys: PartI. The role of curved isotherms on grain selection, MET MAT T A, 31(11), 2000, pp. 2877-2886
The development of crystallographic texture during directional solidificati
on has been quantitatively analyzed in columnar castings of the Ni-base sup
eralloys, CMSX4 and CM186LC, produced with a range of cooling rates and liq
uidus front curvatures. It is proposed that the more diffuse crystallograph
ic texture developed in CMSX4 relative to CM186LC results from a combinatio
n of the differing local orientation stability condition and the alloys' so
lidification characteristics. The implications of these additional factors
on the evolution of the axial grain texture, the grain orientations produce
d in single-crystal processing, and the stability of spurious grains in pro
cessing CMSX4 are discussed. An experimental method is presented to quantit
atively analyze the grain selection process in the case of curved liquidus
isotherms by retaining the stereology of the primary [001] dendrite growth
direction and the local thermal gradient vector. This can account for the s
tability of spuriously nucleated edge grains in a single-crystal matrix.