A direct, simple and one-step synthesis of tetramethylammonium trioxyfluoromolybdate (VI)

Citation
Ar. Mahjoub et al., A direct, simple and one-step synthesis of tetramethylammonium trioxyfluoromolybdate (VI), J CHEM R-S, (10), 2000, pp. 486-487
Citations number
20
Categorie Soggetti
Chemistry
Journal title
JOURNAL OF CHEMICAL RESEARCH-S
ISSN journal
03082342 → ACNP
Issue
10
Year of publication
2000
Pages
486 - 487
Database
ISI
SICI code
0308-2342(200010):10<486:ADSAOS>2.0.ZU;2-V
Abstract
Reaction between tetramethylammonium fluoride (CH3)(4)NF and MoO3 in 1:1 mo lar ratio in the minimum amount of dry acetonitrile gives tetramethylammoni um trioxyfluoromolybdate (VI), (CH3)(4)N[MoO3F] in very high yields. The co mpound has been characterized by elemental analyses and IR spectral studies . The advantages of the new method are discussed.