Jb. Quinn et Ik. Lloyd, Comparison of methods to determine the fracture toughness of three glass-ceramics at elevated temperatures, J AM CERAM, 83(12), 2000, pp. 3070-3076
Two standardized methods for measuring K-Ic in ceramics are compared for us
e at high temperatures (precracked beam and surface crack in flexure). Resu
lts from a third technique involving the measurement of cracks around Vicke
rs indentations are also presented. Three dental glass-ceramics, differing
primarily in microstructure, were used as model materials in this study, Th
ey emphasized the importance of microstructure in determining high-temperat
ure K-Ic values and the challenges in measuring them. The measured fracture
toughnesses decreased with temperature and increased with imbedded grain s
ize for all three methods.