Wide-angle X-ray scattering studies of carbon nanotubes produced by catalyt
ic decomposition of acetylene on a supported Co catalyst are reported. The
X-ray intensities were recorded up to maximum scattering vector K-max = 24
Angstrom and then Fourier transformed to real space. Yielding the radial di
stribution functions of good spatial resolution were analysed by the model
based on fitting procedures method. Detailed analysis of the experimental d
ata by a least-squares fitting procedure shows that the local atomic struct
ure exhibits the expected hexagonal network with the nearest-neighbour C-C
distance of 1.41 Angstrom. Investigation of stacking nature of subsequent l
ayers suggests the structure in which adjacent layers are arranged without
spatial correlations with inter-tubule spacing of about 3.4 Angstrom.