Superconducting YBa2Cu3O7-delta films were grown by resistive evaporation o
n multicrystalline silver film which was evaporated on MgO substrate. A sim
ple inexpensive vacuum system equipped with resistively heated boat was use
d for the whole process. Silver film was first evaporated on MgO substrate
kept at 400 degreesC during the evaporation after which with no further ann
ealing a precursor mixture of yttrium small grains and Cu and BaF2 in powde
r form weighed in the atomic proportion to yield stoichiometric YBa2Cu3O7 w
as evaporated.
The films thus obtained were annealed at 740 degreesC under low oxygen part
ial pressure of about 1Pa for 30 minutes to form the superconducting phase.
X-ray diffraction and scanning electron microscopy techniques were used fo
r texture and surface analysis. Electrical properties were determined using
a standard de four-probe for electrical measurements.
The physical and electrical properties of the YBCO films are discussed in l
ight of the fact that X-ray diffraction measurements done on the silver fil
m have revealed a multicrystalline structure.