The magnetic properties have been examined following the phase separation p
rocess for Cu-rich La2CuO4,003 sample. The ferromagnetic correlation, which
is represented as magnetic hysteresis loop, was found for the first time t
o evolve with the progress of phase separation. It is suggested that the de
tected ferromagnetic correlation is the result of spin polarization embedde
d in the hole-rich region due to phase separation.