Mixed Al+AlN nanoparticles were synthesized by an active plasma-metal
reaction method. Mean particle size of the mixed Al+AlN nanoparticles
is about 30-50 nm. Defects were found in some AIN particles. Moreover,
the AIN ratio and its particle size in mixed Al+AlN nanoparticles obt
ained in different atmospheres (N-2+Ar) increase with increasing N-2 p
article pressure, and the specific surface areas of the mixed Al+AlN n
anoparticles increase with the AIN ratio. The surface degradation of t
he Al+AlN exposed to air is estimated by the infrared absorption spect
ra.