Solid phase microextraction of polycyclic aromatic hydrocarbons from soil

Authors
Seduikiene, I Vickackaite, V Kazlauskas, R
Citation
I. Seduikiene et al., Solid phase microextraction of polycyclic aromatic hydrocarbons from soil, CHEM ANAL, 45(6), 2000, pp. 835-842
Citations number
9
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
CHEMIA ANALITYCZNA
ISSN journal
00092223 → ACNP
Volume
45
Issue
6
Year of publication
2000
Pages
835 - 842
Database
ISI
SICI code
0009-2223(2000)45:6<835:SPMOPA>2.0.ZU;2-I
Abstract
A headspace solid phase microextraction technique for the determination of polycyclic aromatic hydrocarbons in soil is suggested. The optimum extracti on conditions from headspace of the humic soil are: temperature 60 degreesC for 30 min and desorption for 2 min at 250 degreesC.The precision and line arity of determination as well as detection limits for acenaphthene, fluore ne and anthracene were estimated. It was demonstrated that the extraction e fficiency strongly depends on the humidity of the soil.