N. Tanaka et al., PREPARATION OF ALUMINUM NITRIDE EPITAXIAL-FILMS BY ELECTRON-CYCLOTRON-RESONANCE DUAL-ION-BEAM SPUTTERING, JPN J A P 1, 33(9B), 1994, pp. 5249-5254
Aluminum nitride (A1N) thin films have been deposited on (1 $($) over
bar$$ 1.2) sapphire by an electron cyclotron resonance (ECR) dual-ion-
beam sputtering method. We have thoroughly investigated the dependence
of the crystallinity and surface smoothness of the A1N thin film on t
he assisted conditions and sputtering conditions. The A1N thin film de
posited under assisted conditions with the nitrogen ion beam energy an
d current density of 100 eV and 0.32 mA/cm(2), respectively, and sputt
ering conditions with the arrival aluminum flux rate to the substrate
surface (Al flux rate) and argon (Ar) ion beam energy of 42 Angstrom/m
in and 800 eV, respectively, is a single-crystal film with a very smoo
th surface. In order to prepare the epitaxial film, the Ar ion beam en
ergy must be increased according to increases in the Al flux rate, and
decreased according to decreases in the Al flux rate.