Om. Ragg et Ir. Harris, A STUDY OF THE EFFECTS OF THE ADDITION OF VARIOUS AMOUNTS OF CU TO SINTERED ND-FE-B MAGNETS, Journal of alloys and compounds, 256(1-2), 1997, pp. 252-257
Magnets according to the formula (Nd16Fe76B8)(1-x)Cu-x (0.1 less than
or equal to x less than or equal to 1.5) have been produced by adding
Cu powder to hydrogen decrepitated Nd-Fe-B powder prior to ball millin
g, as part of the powder metallurgy processing route. Microstructural
examination of the sintered magnets revealed increasing porosity with
increasing Cu content. Heat treating the sintered magnets at 500 degre
es C increased the coercivities of all of the magnets and in particula
r the magnet with 0.25 at.% Cu, which was found to be the optimum addi
tion. This magnet exhibited a steady increase in coercivity on anneali
ng, without any detrimental effect on the remanence. This enabled a ma
gnet to be produced with a remanence of 1295 mT, an intrinsic coercivi
ty of 1030 kA m(-1) and a maximum energy product of similar to 340 kJ
m(-3) (similar to 43 MG Oe). (C) 1997 Elsevier Science S.A.