Composite SiO2-iron oxide materials were prepared by three experimental pro
cedures. In the first case, the iron oxides were precipitated during a sol-
gel process. In the second case, a SiO2 matrix was initially obtained, and
the iron oxides were formed by thermal treatment after impregnation of a so
luble Fe2+ salt in the previously processed matrix. In the third method, fe
rrite powders, prepared by wet chemical method, were embedded into a SiO2 b
ased sol-gel matrix. Materials with convenient porosity and nano-sized iron
oxide content could be prepared using the mentioned methods. The prepared
composite has been tested for arsenic(V) removal.