F-19, C-13 SINGLE-BOND AND 2-BOND 2D NMR CORRELATIONS IN PERFLUOROHEPTANOIC ACID

Authors
RIBEIRO AA
Citation
Aa. Ribeiro, F-19, C-13 SINGLE-BOND AND 2-BOND 2D NMR CORRELATIONS IN PERFLUOROHEPTANOIC ACID, Journal of fluorine chemistry, 83(1), 1997, pp. 61-66
Citations number
28
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear
Journal title
Journal of fluorine chemistry → ACNP
ISSN journal
00221139
Volume
83
Issue
1
Year of publication
1997
Pages
61 - 66
Database
ISI
SICI code
0022-1139(1997)83:1<61:FCSA22>2.0.ZU;2-4
Abstract
The first F-19, C-13 single- and multi-bond 2D NMR correlations using fluorine detection methods are reported for a perfluorinated alkyl cha in. These heteronuclear correlations are observed in perfluoroheptanoi c acid and combined with F-19-decoupled C-13 data and homonuclear F-19 , F-19 COSY to derive a full set of unequivocal F-19 and C-13 assignme nts. (C) Elsevier Science S.A.