We succeeded in growing highly Fe-doped GaN films by solid-source molecular
beam epitaxy using an electron-cyclotron-resonance microwave nitrogen plas
ma. The substrate temperature was in the range of 380-520 degreesC. The sam
ples were analyzed by x-ray diffraction and transmission electron microscop
y, and showed hexagonal (wurtzite) or cubic (zincblende) structure or a mix
ture of both phases. The Fe concentration was on the order of 10(19) cm(-3)
and extended x-ray absorption fine structure data show that the Fe is subs
tituting the Ga in GaN. The magnetization measurements as a function of tem
perature reveal ferromagnetic properties below 100 K for the sample grown a
t the lowest temperature. (C) 2000 American Institute of Physics. [S0003- 6
951(01)00601-5].