S. Zhu et al., Modified growth of cadmium selenide single crystals from the vapor phase and quality characterization, CRYST RES T, 35(11-12), 2000, pp. 1239-1244
High quality size of CdSe single crystal of large size was obtained by the
modified growth technique, i.e. horizontal vapor phase located point nuclea
tion (HVPLPN). The particular shape of the growth ampoule and less temperat
ure gradients (7-8 K/cm) in the growth interface was used for crystal growt
h. As-grown CdSs crystal was characterized by varied methods including x-ra
y diffraction, SEM and energy dispersive analyzer of x-ray (EDAX) etc. Two
cleavage facts of the (100) and the (110) was found. The crystal has a stoi
chiometry ratio Cd : Se - 0.99 : 1 and the density of dislocation is in the
range of 10(4)-10(3)/cm(2) and the resistivity is about 10(7) Omega cm. Th
e results demonstrated that the quality of the as-grown crystal is good for
applications. Therefore the modified growth technique (HVPLPN) is a promis
ing convenient new method for the growth of high quality CdSe single crysta
ls.