F. Degave et al., Microstructure of GaN epitaxial films grown on (0001) sapphire by chemicalbeam epitaxy as related to buffer growth conditions, J PHYS-COND, 12(49), 2000, pp. 10307-10312
GaN buffer layers of about 20 nm thickness have been deposited on (0001) sa
pphire between 500 and 600 degreesC. The best morphology was found to corre
spond to a deposition made at 560 degreesC Next. different annealing steps
were made between 800 and 920 degreesC in ammonia or UHV. It is revealed th
at a partial desorption of GaN occurs when the buffer is heated up to 900 d
egreesC. In addition. three GaN epilayers of more than 1 mum thickness were
grown on selected buffer layers after annealing. It is shown that the best
results are obtained for a GaN epilayer grown on a buffer layer annealed a
t 900 degreesC in UHV. in agreement with AFM and optical measurements.