Ea. Dikusar et al., Synthesis of secondary acetylenic peroxy alcohols and their acetates from monosubstituted benzaldehydes, RUSS J G CH, 70(5), 2000, pp. 738-744
A series of secondary alkylaromatic acetylenic peroxy alcohols were prepare
d by reaction of lithium peroxy acetylenides with monosubstituted benzaldeh
ydes. Reaction of intermediately formed lithium peroxy alcoholates with ace
tic anhydride gave the corresponding peroxy-containing acetates. The therma
l stability of the synthesized compounds was evaluated by derivatography.