We describe experiments aimed at detecting heat treatment of silcrete,
a siliceous rock of inhomogeneous lithology widely used in prehistori
c Australia. Our samples (N=66) come from eastern New South Wales. Two
methods widely used on other materials are found to be inadequate: sc
anning electron microscope (SEM) analyses allow conflicting interpreta
tions of the same piece of material, while colour changes an too varia
ble to be a reliable indicator. Two other methods are more reliable: i
ncrease in lustre is rare, but clearly indicates heat treatment when i
ts thermal origin is certain; palaeomagnetism assessments of modern (N
=18) and archaeological (N=23) samples show that while the method does
not give false positives, it indicates heating and not necessarily he
at treatment. A combination of palaeomagnetism and lustre assessments
is recommended. (C) 1997 Academic Press Limited.