The anomalous stress peak found at intermediate temperatures has been exami
ned in Fe-25Al and Fe-28Al alloys by hardness testing over a wide range of
temperatures, using a wide range of strain rates, and studying dislocation
structures in samples both slowly cooled as well as rapidly quenched after
deformation. The anomalous stress rise has been found to show little strain
-rate dependence, while the stress peak temperature and the high-temperatur
e range of falling stress has been shown to be highly strain-rate dependent
. There is no clear change of dislocation structure as the yield stress inc
reases, and the stress fall is sometimes associated with [111] superdisloca
tions and other times with [100] dislocations, depending on the strain rate
considered. Such [100] dislocations appear to be created as mobile [111] s
uperdislocations of different Burgers vector react together, which happens
more readily at higher temperatures and lower strain rates, and this probab
ly affects work hardening behaviour and flow stress levels after yield, but
not the yielding process itself. The absence of any clear evidence of a di
slocation pinning process operating during deformation makes it difficult t
o determine the mechanisms responsible for the stress rise and then fall. (
C) 2001 Elsevier Science B.V. All rights reserved.