A p-type device grade silicon wafer was implanted by 1 MeV Ru+ ions to a do
se of 5.67 x 10(16) cm(-2). The microstructures of the as-implanted and ann
ealed samples were studied mainly by analytical transmission electron micro
scopy (TEM) and X-ray diffraction (XRD). The results showed that the implan
tation resulted in a well-defined surface layer of about 910 nm in thicknes
s. The layer was composed of ultra-fine Ru2Si3 crystallites in an amorphous
matrix. After annealing, the inner part of the layer recovered completely
to single crystal Si with nano-scaled Ru2Si3 embedded in it. A similar to 6
60 nm thick polycrystalline region consisting of Si and Ru2Si3 grains was f
ormed at the surface. (C) 2001 Kluwer Academic Publishers.