Redetermination of 4-(phenyl)thiosemicarbazide

Authors
Lynch, DE McClenaghan, I
Citation
De. Lynch et I. Mcclenaghan, Redetermination of 4-(phenyl)thiosemicarbazide, ACT CRYST C, 56, 2000, pp. E587-E587
Citations number
5
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
ISSN journal
01082701 → ACNP
Volume
56
Year of publication
2000
Part
12
Pages
E587 - E587
Database
ISI
SICI code
0108-2701(200012)56:<E587:RO4>2.0.ZU;2-4
Abstract
The structure of the title compound, C7H9N3S, comprises twisted molecules t hat associate via N-H . . .N and N-H . . .S hydrogen-bonding interactions. The dihedral angle between the phenyl ring and the five-membered thiosemica rbazide plane is 67.56 (5)degrees. This structure was previously determined using data from visual estimation of photographic intensity (measurements at room temperature, with R = 0.112).