H. Protzmann et al., Uniformity control of group-III nitrides grown on 5 x 3 inch Al2O3 substrates in Planetary Reactors((R)), J CRYST GR, 221, 2000, pp. 629-634
We report on recent results obtained using an AIX 2400G3HT production-type
Planetary Reactor(R) in the 5 x 3 inch configuration for growth of typical
group-III nitride layer structures consisting of GaN, InGaN and AlGaN. The
optimum reactor geometry has been found by extensive modeling of the reacto
r design. Increased thermal management allows maximum reactor temperatures
above 1400 degreesC. As a consequence of extensive reactor modeling, the pr
ocess transfer from 6 x 2 to 5 x 3 inch configuration was carried out by si
mple scaling of the corresponding process parameters of the 6 x 2 inch conf
iguration. The scaling factor is calculated with respect to the changed rea
ctor geometry. We used optical reflectrometry for in-situ growth control du
ring this process development and could confirm the theoretical scaling req
uirements for obtaining identical growth conditions as compared to the 6 x
2 inch reactor configuration. This is verified by the generation of identic
al reflectance spectrum features. This important issue of in-situ control i
s discussed in detail. The TMGa efficiency could be kept at about 17%. Swit
ching to the 8 x 3 inch configuration, the efficiency increases up to about
27%, which is an improvement of 63% as compared to the 6 x 2 inch configur
ation. (C) 2000 Elsevier Science B.V. All rights reserved.