P. Saravanan et al., Experimental design and performance analysis of alumina coatings depositedby a detonation spray process, J PHYS D, 34(1), 2001, pp. 131-140
The increasing demands for high-quality coatings has made it inevitable tha
t the surface coating industry would put more effort into precisely control
ling the coating process. Statistical design of experiments is an effective
method for finding the optimum spray parameters to enhance thermal spray c
oating properties, In the present investigation, an attempt is made to prod
uce high-quality alumina (Al2O3) coatings by optimizing the detonation spra
y process parameters following a (L16-2(4)) factorial design approach. The
process parameters that were varied include the fuel ratio, carrier gas flo
w rate, frequency of detonations and spray distance. The coating characteri
stics were quantified with respect to roughness, hardness and porosity. The
performance of the coatings was quantitively evaluated using erosion, abra
sion and sliding wear testing. Through statistical analysis of the experime
ntal results, performed by the ANOVA method, the significance of each proce
ss parameter together with an optimal variable combination was obtained for
the desired coating attributes, Confirmation experiments were conducted to
verify the optimal spray parameter combination, which clearly showed the p
ossibility of producing high-quality Al2O3 coatings.