A simple and effective method of evaluating atomic force microscopy tip performance

Citation
Hy. Nie et Ns. Mcintyre, A simple and effective method of evaluating atomic force microscopy tip performance, LANGMUIR, 17(2), 2001, pp. 432-436
Citations number
28
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
LANGMUIR
ISSN journal
07437463 → ACNP
Volume
17
Issue
2
Year of publication
2001
Pages
432 - 436
Database
ISI
SICI code
0743-7463(20010123)17:2<432:ASAEMO>2.0.ZU;2-W
Abstract
The morphology of a surface imaged by dynamic force mode atomic force micro scopy is obtained through an interaction between the probe tip and surface features. When the tip is contaminated and the size of the contaminant is c omparable to the size of the features on the sample surface, artifacts attr ibutable to the contaminant are observed to dominate the image. To reduce t he possibility of effects from such artifacts, the tip performance should b e checked by scanning a reference sample of known surface morphology. We de monstrate a simple and effective method of evaluating tip performance by th e imaging of a commercially available biaxially oriented polypropylene (BOP P) film, which contains nanometer-scale-sized fibers. This sample is approp riate for use as a reference because a contaminated tip will not detect the fiberlike network structure. In addition, BOPP has a soft, highly hydropho bic surface of low surface energy, thus ensuring that the tip will not be d amaged or contaminated during the evaluation process.