Monodisperse micron macroporous polystyrene resins were synthesized with di
fferent crosslinking degrees. The IR ratio of A(980cm-1)/A(790cm-1) was sel
ected to make the working curve and then determine the amount of pendent do
uble bonds in resin. The result was compared with that of Bartholin's measu
rement. A Standard working curve method is very convenient, especially in t
he measurement of moderate and highly crosslinked macroporous resin, it's m
ore accurate.