The first characterisation results on freeze-dried porous silicon are
reported. The freeze drying process is shown to be highly non-destruct
ive. The samples so far obtained on substrates with different doping d
ensity show better morphological, optical and photoluminescence proper
ties. The first structural information on freeze-dried PS have been ob
tained by Raman and transmission electron microscopy techniques. Compa
red with other drying techniques, freeze drying appears to be a simple
and contamination-free method. (C) 1997 Elsevier Science S.A.