Investigation to obtain long Y123 textured bars by vertical MTG process

Citation
S. Marinel et al., Investigation to obtain long Y123 textured bars by vertical MTG process, EPJ-APPL PH, 13(2), 2001, pp. 77-82
Citations number
10
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
EUROPEAN PHYSICAL JOURNAL-APPLIED PHYSICS
ISSN journal
12860042 → ACNP
Volume
13
Issue
2
Year of publication
2001
Pages
77 - 82
Database
ISI
SICI code
1286-0042(200102)13:2<77:ITOLYT>2.0.ZU;2-M
Abstract
The floating zone method is currently used to obtain Y123 melt textured bar s, however the final sample length is always limited by the sample lower pa rt weight which is sustained only by the liquid phase tension surface energ y. Indeed, the basic scheme is to attach the bar only by the upper part and the lower part is totally free. A vertical furnace permits then to heat lo cally the bar and to create the floating zone. The sample translation at lo w speed (about 1 mm/h) allows the formation of a re-crystallization zone, a ccording to the well known reaction Y211+Liquid (Ba and Cu rich) --> Y123, permitting the fabrication of a well textured bar. This work is devoted to present a modification of this process in order to have no limitation in th e sample length. The idea which is developed here is to include inside the bar and co-axially a platinum wire. We have chosen a platinum wire due to i ts high melting temperature and its relatively low reactivity with Y123. We present here results obtained in term of reactivity, texture formation and superconducting properties when Y123 is textured in the presence of platin um wire versus different doped element introduced in the initial mixture.