In this study, a new methodology for surface modification of food fibers is
proposed via a dry particle coating technology. Basically, in the dry part
icle coating processing, a mechano-chemical reaction between hydrophilic OH
groups of food fiber and silanol groups-Si(OH)-on the surface of hydrophil
ic silica is used, As a result of this reaction, dehydration (H + OA --> H2
O) is expected, leading to suppression of the hygroscopic properties of foo
d fibers for the purposes of better handling and enhancement of the preserv
ative property. For the dry particle coating, a horizontal particle Composi
te equipment with an ellipse shaped rotor was used. The surface of the food
fiber was coated with a very fine hydrophilic silica (SiO2) and a mechano-
chemical reaction,vas activated by a high shear stress and an impaction for
ce in the equipment. The coated powders were prepared under various operati
ng parameters of vessel rotational speed and operation time. The surface pr
operties of the coated powders were evaluated by angle of repose (flowabili
ty), specific surface area, particle size, and a scanning electron microsco
py (SEM) observation. The hygroscopic property was analyzed using a water a
dsorption method in a temperature and humidity controlled chamber. Interact
ion between OH and silanol groups was analyzed by a Fourier Transform Infra
red Spectroscopy (FT-IR) method.
As a result, the optimum operating conditions for preventing hygroscopic pr
operty of food fiber can be determined and the mechanism of the mechano-che
mical reaction can be elucidated.