Improved scalar shift correlation NMR spectroscopy in solids

Authors
Heindrichs, ASD Geen, H Giordani, C Titman, JJ
Citation
Asd. Heindrichs et al., Improved scalar shift correlation NMR spectroscopy in solids, CHEM P LETT, 335(1-2), 2001, pp. 89-96
Citations number
25
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
CHEMICAL PHYSICS LETTERS
ISSN journal
00092614 → ACNP
Volume
335
Issue
1-2
Year of publication
2001
Pages
89 - 96
Database
ISI
SICI code
0009-2614(20010216)335:1-2<89:ISSCNS>2.0.ZU;2-E
Abstract
New isotropic mixing sequences suitable for scalar correlation experiments in solids have been designed using symmetry principles similar to those emp loyed in the construction of the C7 dipolar recoupling sequence. Compared w ith existing methods, the new isotropic mixing sequences are appropriate fo r use with faster MAS rates and show improved magnetization transfer effici encies For carbon-13. (C) 2001 Elsevier Science B.V. All rights reserved.