First experimental results of fluorescence microtomography with 6-mum resol
ution obtained at ESRF, Grenoble, France, are described. The setup comprise
s high-quality optics (monochromator, mirror, focusing lenses) coupled to t
he high-energy/brilliance/coherence of the ID 22 undulator beamline. The to
mographic setup allows precise measurements in the "pencil-beam" geometry.
The image reconstruction is based on a modification of the algebraic recons
truction method but includes simplifications of the model. The quality and
precision of the two-dimensional reconstructed elemental images of a phanto
m sample are encouraging. The method will be further refined and applied fo
r the analysis of more complex inhomogeneous samples.