We describe a method of combining the stabilization of impurities in super-
fluid helium and magnetic resonance techniques to study hyperfine resonance
in atomic deuterium, obtained by passing a D-D-2-HE gas mixture through a
radiofrequency discharge, The resulting D-D-2-He gas mixture penetrates a s
uperfluid helium surface and forms a Van der Waals solid mixture containing
atoms of D and Nr! as well as D-2 molecules, In preliminary experiments we
have applied magnetic resonance (309 MHz) to the beta-delta transition to
study spin-spin and spin-lattice relaxation in atomic deuterium and to prov
ide information about the surroundings of atomic deuterium isolated in the
D-D-2-He solid.