Sp. Lee et al., Effect of fabricating temperature and volume fraction of Nb sheet on impact properties of Nb/MoSi2-ZrO2 laminate composites, J JPN METAL, 64(12), 2000, pp. 1245-1251
Nb/MoSi2-ZrO2 laminate composites have been successfully fabricated by alte
rnately stacking MoSi2-ZrO2 powder layer and Nb sheet, followed by hot pres
sing in a graphite mould. The selected fabricating parameters were hot pres
s temperature and volume fraction of Nb sheet. The instrumented Charpy impa
ct test was carried out at the room temperature in order to investigate the
relationship between impact properties and fabricating conditions. The int
erfacial shear strength between MoSi2-ZrO2 and Nb, which is associated with
the fabricating temperature and the growth of interfacial reaction layer,
is also discussed. The plastic deformation of Nb sheet and the interfacial
delamination were macroscopically observed. The Nb/MoSi2-ZrO2 laminate comp
osites had the maximum impact value when fabricated at 1623 K, accompanying
the increase of fracture displacement and crack propagation energy. The im
pact value of Nb/MoSi2-ZrO2 laminate composites dramatically increased with
increasing the volume fraction of Nb sheet and showed 64.9 kJ/m(2) for Nb
content of 15 vol%. The interfacial shear strength of Nb/MoSi2-ZrO2 laminat
e composites increased with the growth of interfacial reaction layer, which
resulted from the increase of fabricating temperature. It is useful to pro
mote an appropriate interfacial shear strength for the enhancement of impac
t value of Nb/MoSi2-ZrO2 laminate composites. A large increase of interfaci
al shear strength restrains the plastic deformation of Nb sheet.