A. Dominguez-rodriguez et al., Current understanding of superplastic deformation of Y-TZP and its application to joining, MAT SCI E A, 302(1), 2001, pp. 154-161
A review of the high-temperature, steady-state creep of yttria tetragonal z
irconia polycrystals (Y-TZP) as a function of grain size, strain rate, stre
ss, and temperature will be presented in this paper. Data have been analyze
d using the standard creep equation incorporating a threshold stress. Micro
structural observations of deformed samples indicated that deformation was
achieved primarily by grain boundary sliding (GBS). This microscopic charac
teristic was used to join pieces of these materials. When two pieces of cer
amics are compressed in the superplastic regime, GBS will produce a junctio
n between the pieces. Several types of strong junctions have been produced,
i.e. between pieces of the same material having different grain sizes, and
between pieces of different materials. Scanning electron microscopy of the
interfaces showed that each interface was cavity- and crack-free. Vickers
indentations and high-temperature mechanical tests indicated that the inter
faces were as strong as the matrix. This joining technique allows the const
ruction of a complex shape or a functional gradient material. (C) 2001 Else
vier Science B.V. All rights reserved.