Crystallographic characterization of sputter-deposited epitaxial Nb-Cu-Co and Nb-Cu-permalloy multilayers using electron back-scatter diffraction patterns
R. Loloee et al., Crystallographic characterization of sputter-deposited epitaxial Nb-Cu-Co and Nb-Cu-permalloy multilayers using electron back-scatter diffraction patterns, PHIL MAG A, 81(2), 2001, pp. 261-273
Epitaxial Nb-Cu-Co and Nb-Cu-Permalloy(TM) (Py) multilayers have been grown
on (11 (2) over bar0) sapphire substrates by sputter deposition. Electron
backscatter diffraction patterns (EBSPs) have been used to characterize 'in
dividual layers, while atomic force microscopy was used for studying the su
rface topography. EBSPs have been demonstrated to be a viable technique for
characterization of these thin sputtered films. EBSP results have shown th
at the Nb films grow as high quality epitaxial single crystals with (110)(b
cc), orientations. Cu films grown on the epitaxial Nb display two in-plane
epitaxial variants corresponding to two stacking sequences of {111}(fcc) pl
anes. These Cu variants take up the Nishiyama-Wasserman orientation relatio
nship with the underlying Nb. Subsequent sputtering of Co or Fy on the epit
axial Cu films results in the growth of two variants of 111(fcc) layers. Or
ientation maps of the Cu, Co and Py films, which illustrate the size and di
stribution of the growth variants, are presented.