B. Baufeld et al., FERROELASTICITY OF T-ZIRCONIA .2. IN-SITU STRAINING IN A HIGH-VOLTAGEELECTRON-MICROSCOPE, Journal of the American Ceramic Society, 80(7), 1997, pp. 1699-1705
The ferroelastic deformation of t'-ZrO2, the microstructure of which w
as described in detail in Part I, was investigated by in situ deformat
ion experiments in the high-voltage electron microscope at 1150 degree
s C. During the experiments those two domain. variants with their c-ax
es perpendicular to the [010] tensile direction were transformed into
the third one with its c-axis parallel to the tensile direction, The s
ubsequent 'switching' of the domains inside the colonies proceeds much
faster than the penetration of the transformation front into a neighb
oring colony. Therefore, the transformed region, exhibiting a unique t
etragonal structure and containing residual defects, preferentially ex
pands into the longitudinal directions of the colonies. The transforma
tion of single domains proceeds instantaneously within the time resolu
tion of the video tape recording.