The atomic arrangement and conductance during the separation process of gol
d point contacts were simultaneously observed in situ by high-resolution tr
ansmission electron microscopy. One-dimensional arrangements of gold single
atoms, i.e., atomic wires, appeared between two tips at the point contacts
. They were stable when their length was increased up to 2.6 nm. The intera
tomic distance of the wires was 0.25-0.31 nm. Ir was found that metal-insul
ator transition occurs in the wires.