Crystal structure of 1,2-bis(dicyclohexylphosphino)-ethane rhodium(I)-norborna-2,5-diene tetrafluoroborate, C33H56BF4P2Rh and of 1,2-bis(dicyclohexylphosphino)-ethane rhodium(I)-(Z,Z)-cycloocta-1,5-dieue tetrafluoroborate, C34H60BF4P2Rh center dot 1/2CH(3)OH

Authors
Kempe, R Spannenberg, A Drexler, HJ Heller, D
Citation
R. Kempe et al., Crystal structure of 1,2-bis(dicyclohexylphosphino)-ethane rhodium(I)-norborna-2,5-diene tetrafluoroborate, C33H56BF4P2Rh and of 1,2-bis(dicyclohexylphosphino)-ethane rhodium(I)-(Z,Z)-cycloocta-1,5-dieue tetrafluoroborate, C34H60BF4P2Rh center dot 1/2CH(3)OH, Z KRIST-NEW, 216(1), 2001, pp. 165-168
Citations number
5
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES
ISSN journal
14337266 → ACNP
Volume
216
Issue
1
Year of publication
2001
Pages
165 - 168
Database
ISI
SICI code
1433-7266(2001)216:1<165:CSO1R>2.0.ZU;2-8
Abstract
C33H56BF4P2Rh, orthorhombic, Pna2(1) (No. 33), a =18.829(4) Angstrom, b = 1 0.142(2) Angstrom, c = 17.411(3) Angstrom, V = 3324.9 Angstrom (3), Z= 4, R -gt(F)= 0.033, wR(all)(F-2)= 0.089, T= 200 K. C34.50H62BF4O0.50P2Rh, monoclinic, P12(1)/cl (No. 14), a = 20.009(4) Angstr om, b = 10.335(2) Angstrom, c = 19.638(4) Angstrom, beta = 114.51(3)degrees , V=3695.1 Angstrom (3), Z = 4, R-gt(F)=0.046, wR(all)(F-2) = 0.127, T = 20 0 K.