An array of nickel nanowires enveloped in polyaniline nanotubules was prepa
red by the "second-order-template" method. As the first step, an array of t
he polyaniline nanotubules was synthesized in the pores of an alumina membr
ane, then nickel nanowires were fabricated by electrochemical deposition of
the nickel into the polyaniline nanotubules. The composite nanostructure w
as characterized by x-ray powder diffraction, and scanning electron microgr
aphy. Its magnetic properties were measured by a vibrating sample magnetome
ter. The coercivity and remanence are of high anisotropy with a maximum at
theta =90 degrees (parallel to the nanowires). (C) 2001 American Institute
of Physics.