X-ray absorption spectra near K edges of Pb (88.0keV) and Pt (78.4keV) for
the foils were measured in transmission mode at SPring-8. We succeeded for
the first time in observing the EXAFS oscillation of the Pb foil at 12K, al
though it was failed at room temperature in a previous experiment. The ampl
itude of the EXAFS oscillation of the Pt foil at 12K considerably increased
in comparison with that at room temperature, indicating that the amplitude
is very sensitive to the Debye-Waller factor at high-k values.