Mdm. Innocentini et Vc. Pandolfelli, Permeable porosity of refractory castables evaluated by the water-expulsion porosimetry technique, J AM CERAM, 84(1), 2001, pp. 236-238
In this work, the water-expulsion porosimetry technique was used to quantif
y the permeable pores of self-flow ultralow-cement refractory castables tha
t were treated at 600 degrees -1650 degreesC. Results have shown that the m
ethod as proposed in previous works was not valid, because water was not re
moved continuously from pores, relative to increased pressure, Nevertheless
, the maximum pore diameter obtained according to ASTM Method E128-89 could
be successfully correlated with other castable physical properties (such a
s the permeability constants from the Forchheimer equation) and the apparen
t porosity obtained via the Archimedes technique. Although the apparent por
osity decreased as the thermal treatment temperature increased, the pore mo
rphology changed continuously, with the generation of less-tortuous and mor
e-permeable paths for fluid flow.