P. Parrilla et Jlm. Vidal, DETERMINATION OF PESTICIDE-RESIDUES IN WATER USING LLE OR SPE AND HPLC DAD DETECTION/, Analytical letters, 30(9), 1997, pp. 1719-1738
A comparative study was carried out to determine 21 pesticides in envi
ronmental water samples by high performance liquid chromatography usin
g both liquid-liquid (LLE) and solid-phase (SPE) extractions. The repr
oducibility of the SPE method is better than employing LLE with dichlo
romethane, but SPE was more efficient to recover metomyl, dimethoate,
chlorpyrifos ethyl and carbophenothion.