Reducing chemical vapour infiltration time for ceramic matrix composites

Citation
La. Timms et al., Reducing chemical vapour infiltration time for ceramic matrix composites, J MICROSC O, 201, 2001, pp. 316-323
Citations number
6
Categorie Soggetti
Multidisciplinary
Journal title
JOURNAL OF MICROSCOPY-OXFORD
ISSN journal
00222720 → ACNP
Volume
201
Year of publication
2001
Part
2
Pages
316 - 323
Database
ISI
SICI code
0022-2720(200102)201:<316:RCVITF>2.0.ZU;2-4
Abstract
Conventional routes to producing ceramic matrix composites (CMCs) require t he use of high temperatures to sinter the individual ceramic particles of t he matrix together. Sintering temperatures are typically much higher than t he upper temperature limits of the fibres. This paper details preliminary w ork carried out on producing a CMC via chemical vapour infiltration (CVI), a process that involves lower processing temperatures, thus avoiding fibre degradation. The CVI process has been modified and supplemented in an attem pt to reduce the CVI process time and to lower the cost of this typically e xpensive process. To this end microwave-enhanced CVI (MECVI) has been chose n, along with two alternative pre-infiltration steps: electrophoretic infil tration and vacuum bagging. The system under investigation is based on sili con carbide fibres within a silicon carbide matrix (SiCf/SiC). The results demonstrate that both approaches result in an enhanced initial density and a consequent significant reduction in the time required for the MECVI processing step. Dual energy X-ray absorptiometry was used as a nond estructive, density evaluation technique. Initial results indicate that the presence of the SiC powder in the pre-form changes the deposition profile during the MECVI process.