Detailed description of a compact cryogenic magnetic resonance force microscope

Citation
Dd. Smith et al., Detailed description of a compact cryogenic magnetic resonance force microscope, REV SCI INS, 72(4), 2001, pp. 2080-2089
Citations number
45
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences","Instrumentation & Measurement
Journal title
REVIEW OF SCIENTIFIC INSTRUMENTS
ISSN journal
00346748 → ACNP
Volume
72
Issue
4
Year of publication
2001
Pages
2080 - 2089
Database
ISI
SICI code
0034-6748(200104)72:4<2080:DDOACC>2.0.ZU;2-Y
Abstract
We describe the design and operation of a cryogenic magnetic resonance forc e microscope for detecting nuclear magnetic resonance. Instrument-critical details are enumerated, including fabrication of a positionable radio-frequ ency coil, detection of angstrom-level microcantilever oscillations using a n optical fiber interferometer, design of a compact fiber/cantilever alignm ent system, temperature compensation of the fiber/cantilever gap, control o f sample temperature, and vibration isolation. Additionally, experimental p rotocols and sample specific considerations such as spin relaxation times a re addressed. F-19 nuclear magnetic resonance data obtained from a Nd-doped CaF2 sample are presented.